| Title: | Method for preparing quasi-ginsenoside P11 | ||
| Application Number: | 99122505 | Application Date: | 1999.11.08 |
| Publication Number: | 1251369 | Publication Date: | 2000.04.26 |
| Approval Pub. Date: | Granted Pub. Date: | 2004.08.11 | |
| International Classifi-cation: | C07J17/00 | ||
| Applicant(s) Name: | Shenyang Medicine Univ. | Address: | 110015 |
| Inventor(s) Name: | Li Xi, Wang Jinhui | ||
| Attorney & Agent: | li yutong | ||
|
|
|
||
Abstract: |
|||
| The preparation method of pseudoginsenoside F11, suitable for industrial production, adopts the following steps: using water (or dilute alcohol) to extract American ginseng stem and leaf; n-butanol-water liquid-liquid extraction (or alcohol precipitation) of extract; making the n-butanol extracted portion (or aqueous solution produced after precipitation) is conducted macroporous resin and water elution to remove sugar and protein, and alcohol washing to obtain total saponin; then using silica gel chromatography to treat said total saponin to obtain crude product of said compound; finally, refining said crude product by utilizing methanol recrystallization (or high-performance liquid chromatography) to obtain the invented product. | |||
|
|
|||
| Time: | 4 | ||
<- Previous Patent:3 beta-hydroxy-5-cholenic acid es...
| Next Patent:High-stereoselectivity synthesiza... ->
|
|||