Process for synthesizing 1-n-butyl azetidene-2-one
In this invention, orthobutanol, potassium (or sodium) bromide, H2SO4 are used as raw materials to generate orthobrombutane, and the orthobrombutane (or benzyl chloride) and caprolactam ...
2
90103105
Synthesis process of permeate agent azoen
The present invention relates to a synthesizing process of osmosizing agent (A zone) capable of promoting conveying drug into inner layer of human or animal skin and quickening skin abso...
3
90103295
Therapeutic agents
The compound of formula below and its salt may be used as blood sugar dropping agent. In the formula below: n=0 or 1; R1 and R2 represents aliphatic group or naphthenic group; or NR1R2 r...
4
90103419
Z-hydroxyl quinoline preparation method
Said invention provided with two steps synthesis method for praparation of quinolone using ortho-phenyl enenediamine and chloro acetic acid as raw material, and ammonium carbonate as aci...
Process for preparing phylloporphyrin
This phylloporphyrin prepared according to this invention is a photosensitive agent as a medicine for laser diagnosis. Under the radiation of laser, it shows red fluorescence at positive...
Indole derivatives
Compounds are disclosed of formula wherein R1 represents a C1-6 alkyl group; R2 represents a hydrogen atom or a C1-3 alkyl group; n represents zero or an integer from 1 to 3; and pharmac...
Preparation of new type amide compound with xanthic surface
By extaction from the leaves of clausena lansium, separation and purification, two clausena-amide compounds with following molecular formulas are obtained, which are effective on curing ...
11
90107375
Synthesizing method of tetrachloroquinone anhydride
The present invention relates to a method for synthesizing tetrachlorobenzene anhydride which is used in fine chemical industry. It is to use chlorosulfonic acid as reaction solvent, iod...
12
90106365
Cantharidin fat-soluble medicament preparation
The present invention relates to a fat-soluble cantharidin intermediate preparation and a method for preparing a series of antiviral and antibiotic new preparation wherein the prepared i...
Asymmetric epoxidation using chiral hydroperoxide
Prochiral ethylenically unsaturated substrates are converted to chiral epoxides by reaction with optically active hydroperoxides in the presence of transition metal catalysts. For exampl...
18
90109457
Alkylene oxide catalysts containing high silver content
Catalysts for the epoxidation of alkene, esp. ethylene, to the corresponding alkylene oxide, e.g., ethylene oxide, which catalysts contain a high silver content on carriers having a high...
Extracting bilirubin from bible with double-stablizing method
This invention discloses an improved process for preparing cholerythrin from animal's bile. A mixed solvent of ethyl acetate and dichloromethane is added to the bile to extract free chol...
Method for extracting natural caffeine from tea
The present invention refers to a method for extracting natural caffeine from tea. A non-toxic organic solvent is mixed with tea in the specified proportion and heated, then separated ce...
24
90109981
Preparation of alcohol-extended and amine-extended piperazines
A process for preparing alcohol-extended and amine-extended piperazines comprising contacting a difunctional aliphatic alcohol with a reactant amine, wherein at least one of the aliphati...
25
91100048
Synthetic method of 4-hydroxy-7-chloro-quinolinic acid
This synthetic process of 4-hydroxy-7-chloro-Quinolinic acid is an organic synthetic technology which aims at solving the problems existed in existing processes, such as high consumption...
26
91100370
Purification method of L-proline
The present invention relates to a purification method of L-proline. The existent L-proline purification methods, including ion-exchange resin method, ethyl alcohol-ethyl ether method an...
27
91100760
Extraction of berberin by salting out with biacid
The present invention refers to a method for extracting Coptis chinensis by soaking with two acids and salt. It uses root of phellodendron amurense tree as main raw material, which is fi...
28
91100541
Synthesis method for Bentazon herbicide
This invention relates to process for preparing a kind of herbicide. The easily getting isatin anhydride is used as raw material, which is reacted with a solvent such as dichloro-ethane,...
Synthetic method for photosensitive material couplant AP
The present invention discloses a method for synthesizing non silver salt couplant AP which is an international novel organic photosensitive material developed quickly in recent years, t...
31
92109524
Acridine derivatives
Compound with general formula described in specification, its salt and solution are disclosed. The said compound can make cancer cells resisting the action of several pharmaceuticals sen...
Technology for extracting natural caffeine from tea
This process to extract natural coffeine from tea leaves includes steam-cooking tea leaves, filtering and centrifugal dewatering steps. It keys are as follows: further concentrating tea ...
34
92109618
Process for producing flavone compounds from skullcap (root)
This invention relates to a process to extract flavonoid from a Chinese herbal medicine, skullcap root. Its technological steps include decocting skullcap root twice, filtering, merging ...
35
92106681
Process for producing 5-fluoropyridine derivatives
Process to prepare 5-fluoropyridine derivatives is that correspondent fluoro-acetate is condensated with formate by use of sodium alkoxide as condensating agent and then cyclized with bu...
Process for preparing N-(tetrahydrofuran-2-formyl) piperazine
N-(tetrahydrofuran-2-formyl) piperazine that is a key intermediate during preparing an antihypertension medicine is prepared by reaction of tetrahydrofuryl-2-formyl chloride with piperaz...
3-piperidinylmethylcarboxylate substituted indoles
A process to prepare indole derivative, quaternary ammonium derivative, piperidine N-oxide, and pharmacologically acceptable salt and solvate of a compound with formula described in pres...
42
92110360
Process for preparation of benzimidazole compound
The present invention relates to a preparation method of benzimidazole compound. It is made up by using acetoaminophenol as the raw material and making that pass through the processes of...
43
92109852
Preparing technology for rubber vulcaniztion promoter
A kind of novel one-step synthesis process for production of N-tert-butyl-2-benzothiazole-hyposulfamide. The features is that the thiol-benzothiazole, approprite amount of water and non-...
44
92110282
Heterocyclic compounds
Heterocyclic compound with a structural formula described in specification is an antibiotic predn. for oral application.
45
92110157
Preparation of dihydropyridine derivative
The present invention relates to a dihydropyribine derivative. This compound can prevent calcium ion from inward flowing into cell, and has the notable functions of dilating blood vessel...
46
92110301
Process for purification of hematoidin
This invention relates to a preparing method of bilirubin. It involves bile sucking, primary products preparing, stratified separating out, recovery of distillation, separating out choli...
47
92110017
Heterocyclic compounds
Heterocyclic compound, its salts and metabolism-unstable ester and solvent, and their preparing processes are disclosed. Said heterocyclic compound has a general chemical formula describ...
Z'Z'-di-delta to the power 2-oxazoline synthetic process
Process to prepare 2,2'-bis- delta (2)-oxazoline by cyclization reaction of bis-beta-chloroethyl oxamide features that cyclization reaction takes place in alkaline methanol or alcohol so...
Benzopyranes as potassium channel openers The present invention relates to compounds of formula (I) and the pharmaceutically acceptable salts thereof, wherein the dashed line represents an optional covalent bond; X is O, NH, S or...
52
94191430
Process for preparing acryl-piperidine carbinols A process for the preparation of a compound of formula (I) in which R3 is hydrogen, C1-6 alkyl or C1-6 alkylaryl, by using diborane, of a compound of formula (II), in which R3 is as defin...
53
94191580
Process to prepare herbicidal bicyclic triazoles The invention relates to a process to prepare compounds of Formula (I), wherein Q and Z are defined within. This invention also relates to intermediates of Formula (II) and (IV), wherein ...
Crystalline ceftiofur free acid Crystalline free acid form of the cephalosporin antibiotic ceftiofur (I), processes for its manufacture, and pharmaceutical compositions containing it are provided.
56
94191805
Method and apparatus for extracting taxol from source materials Method and apparatus are described for isolating natural therapeutic compositions from source materials. The method and apparatus isolate natural therapeutic compositions from waxes and o...
57
94103014
Process for preparing pyrrolizine derivaties
The invention relates to the method for preparation of 5-aroyl-2,3-dihydro-1H-dipyrrole-1,1-dicarboxylic ester and its intermediates.
Dihydrobenzofuran derivatives, their production and use There are disclosed novel dihydrobenzofuran derivatives of the formula: (I) wherein A, X, Y, Z, R1 and R2 are each as defined in the description. Also disclosed are a herbicidal compositi...
Method for purifying taxoids A method for purifying taxoids (Taxotère, 10-deacetylbaccatin III) by centrifugal partition chromatography.
66
94191613
Imidazoloquinoxalinone derivatives as eaa antagonists Described are imidazoloquinoxalinones of the formula (I) in which A and R1 to R6 are as defined in the description, plus their preparation. The compounds described can be used to control ...
Tetracyclic compounds as dopamine agonists A tetracyclic compound of formula (I) wherein A and the atoms to which it is attached and the optional double bond represent a mono- or di-heterocyclic ring selected from formulas (a), (b...
Photochromic naphthopyran compounds A naphthopyran compound of general formula (I) wherein R1 represents a group of the formula -NR2R3 wherein each of R2 and R3, which may be the same or different, independently represents ...
76
94192113
4-arylisoindole analgesics The 4-arylisoindoles of the formula (I)are effective analgesics including stereoisomers and pharmaceutically acceptable salts thereof, wherein (II) is (III), (IV) or (V); with the proviso...
Substituted 1-aryltriazolinones The invention relates to novel substituted 1-aryltriazolinones of the general formula (I). The invention also concerns preparation method and their intermediates,and their use as herbicid...
79
00101036
Process for preparation of amino-triazine The present invention relates to a process for the preparation of aminotriazine derivatives of the formula I by the solvolysis of compounds of the formula II in the presence of gaseous hy...
Method for preparing tetrahydro-carbazolone derivative
The process for peparing a medical heterocyclic compound, tetrahydro-carbazolone derivative features simple method, shorter preparing period and mild reaction condition.
82
94103732
Sulfonamido heterocyclic thrombin inhibitors
The invention provided a kind of thrombin inhibitor sulfonamido heterocycle having structure as shown, it includes all its stereo isomer and salt, where symbols n, G, R, R1, R2, R3 and R...
Pyrazole derivative Pyrazole compounds of formula [1] and their tautomers and salts: [1] (wherein R1 is an alkyl group, etc.; R2 is a carboxyl group, etc.; R3 is a halogen atom, an alkyl group, a phenyl grou...
Method for preparation of 4-hydroxy coumarin
The method for preparation of 4-hydroxy-coumarin is that the intramolecular cleisen condensation reaction is conducted by using methyl acetyl-salciylate as raw material, liquid paraffin ...
Dimethylfurancarboxanilide derivative
A dimethylfurancarboxanilide derivative of general formula wherein R1 and R2 may be the same or different from each other and each represent hydrogen, C2-C6 alkyl, C3-C6 cycloalkyl, C3-C...
97
94192180
Herbicidal (4-substituted pyridyl)-3-carbinols (4-substituted pyridyl)-3-carbinols of formula (I), wherein R is hydrogen, or an acyl, alkyl or carbamyl group exhibit desirable preemergent and postemergent herbicidal activity. Also dis...
98
94112129
Protein and polypeptide mercapto-polyglycol (PEG) reagent
The PEG reagent, N-maleimide amino n-caproic acid-mPEG ester, is used for modifying solubility, stability and immunogen nature of protein and polypeptide and also for preparing medical P...
99
94191934
Risperidone pamoate The invention relates to a compound which is a pamoate acid addition salt of risperidone, compositions comprising the same and processes for preparing said compound and compositions.